Sample Preparation Handbook for Transmission Electron Microscopy: Techniques

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This two-volume Handbook is a comprehensive guide to sample preparation for the transmission electron microscope. Sample Preparation Handbook for Transmission Electron Microscopy: Techniques describes 14 different preparation techniques, including 22 detailed protocols for preparing thin slices for TEM analysis. Compatibility and pre-treatments are also discussed. Experimental conditions and guidelines, options and variations, advantages and constraints, technical hints from the authors’ years of experience, common artifacts, and theoretical issues are all considered. Particular attention is given to the type of material, conditioning, compatible analysis of a given preparation, and risks. This practical and authoritative reference companion deserves a place on the bench in every TEM lab.

Key Features of the Handbook:

  • Combines all of the latest techniques for the preparation of mineral to biological samples
  • Compares techniques in terms of their application areas, limitations, artifacts, and types of analysis (macroscopic, atomic, or molecular level)
  • Describes physical characteristics, chemistry, structure/texture, and orientation properties of materials in relation to the most appropriate type of TEM analysis
  • Links to a complementary interactive database website which is available to scientists worldwide*
  • Written by authors with 100 years of combined experience in electron microscopy

*http://temsamprep.in2p3.fr/

Author(s): Jeanne Ayache, Luc Beaunier, Jacqueline Boumendil, Gabrielle Ehret, Danièle Laub (auth.)
Edition: 1
Publisher: Springer-Verlag New York
Year: 2010

Language: English
Pages: 338
Tags: Characterization and Evaluation of Materials; Biological Microscopy; Mineralogy; Nanotechnology

Front Matter....Pages i-xxv
Techniques: General Introduction....Pages 1-4
Preliminary Preparation Techniques....Pages 5-106
Thinning Preparation Techniques....Pages 107-152
Mechanical Preparation Techniques....Pages 153-228
Replica Techniques....Pages 229-256
Techniques Specific to Fine Particles....Pages 257-275
Contrast Enhancement and Labeling Techniques....Pages 277-316
Back Matter....Pages 317-338