The state-of-the-art in NMR spectral analysis. This interactive tutorial provides readers with a comprehensive range of software tools and techniques, as well as the necessary theoretical knowledge required to analyze their spectra and obtain the correct NMR parameters. Modern Spectral Analysis provides expert guidance, by presenting efficient strategies to extract NMR parameters from measured spectra. A database of selected spectra and modern, powerful WIN-NMR software designed by Bruker are provided on the enclosed CD-ROM. The programs provided are 1 D WIN-NMR, WIN-DAISY, WIN-DR and WIN-DYNAMICS, and direct data exchange between all these programs is possible. Readers are shown how they can obtain maximum structural information from their 1 D NMR spectra with time-saving computer assistance. Practical problems that can occur and their solutions are discussed at length using clear, easy-to-follow examples. Both homo- and heteronuclear and first- and second-order spin systems are demonstrated. Moreover, relaxation analysis, nuclear Overhauser effects and magnetic site exchange are all covered in this hands-on guide to NMR spectral analysis.
Author(s): Ursula Weber
Series: Spectroscopic Techniques: An Interactive Course
Edition: Har/Cas
Publisher: Wiley-VCH
Year: 1998
Language: English
Pages: 411
Tags: Химия и химическая промышленность;Аналитическая химия;Физические методы анализа;ЯМР-спектроскопия;
Cover Page......Page 1
Title: NMR Spectroscopy: Modern Spectral Analysis......Page 4
ISBN 3527288287......Page 5
Preface......Page 6
Acknowledgments......Page 13
Table of Contents (with page links)......Page 14
1.1 Scope and Audience......Page 18
1.2 Organisation......Page 19
1.3 Personal Qualifications......Page 21
1.4 Contents......Page 22
1.5 Technical Requirements......Page 24
1.6 Software......Page 25
1.7 Recommended Reading and References......Page 33
2 General Characteristics of Spin Systems......Page 36
2.1 The Chemical Shift......Page 37
2.2 First Order Spin Systems......Page 53
2.3 Second Order Spin Systems......Page 80
2.4 Magnetic Equivalence......Page 115
2.5 References......Page 146
3.1 Symmetry Effects......Page 148
3.2 Configuration Isomers in NMR......Page 177
3.3 Conformation and NMR......Page 192
3.4 References......Page 245
4.1 Spin=1/2 Pure Elements......Page 246
4.2 Spin-1/2 Rare Isotopes......Page 276
4.3 Spin Systems with Quadrupolar Nuclei......Page 310
4.4 References......Page 331
5.1 Relaxation Times......Page 334
5.2 Nuclear Overhauser Effect......Page 344
5.3 Magnetic Site Exchange......Page 356
5.4 References......Page 378
6.1 Quantum Mechanical Theory......Page 380
6.2 Spin Spin System Probabilities......Page 393
6.3 The Lineshape Fitting......Page 395
6.4 Glossary......Page 399
6.5 References......Page 401
Index (with page links)......Page 402
Back Page......Page 411
