Cover......Page 1
COSY Spectra-Quantitative Analysis......Page 2
Quantitative Measurements......Page 10
Adsorbed Species -Spectroscopy and Dynamics......Page 20
Bronsted Acidity of Solids......Page 26
Chemical Exchange on Solid Metal Surfaces......Page 32
Cokes......Page 37
Diffusion in Porous Media......Page 43
Microporous Materials and Xenon-129 NMR......Page 51
Molecular Sieves- Crystalline Systems......Page 58
Reactions in Zeolites......Page 75
Silica Surfaces- Characterization......Page 82
Supported Metal Catalysts......Page 98
Vanadium Catalysts- Solid State NMR......Page 111
Chemical Exchange Effects on Spectra......Page 124
Chemical Exchange on Solid Metal Surfaces......Page 134
Dynamic NMR in Liquid Crystalline Solvents......Page 139
Dynamics in Solid Organic Compounds-Intramolecular Motions......Page 154
Dynamics of Hydrogen Transfer in Liquids and Solids......Page 163
Fluxional Motion......Page 175
Gas Phase Studies of Chemical Exchange Processes......Page 187
Kinetics at High Pressure......Page 193
Magnetic Equivalence......Page 202
Molten Salts......Page 213
Relaxation Effects of Chemical Exchange......Page 217
Reorientation in Crystalline Solids- Propeller-Like R3M Species......Page 228
Structural and Dynamic Characterization of Soft Polymers by Solid State NMR and Field Gradient NMR......Page 234
Two-Dimensional Methods of Monitoring Exchange......Page 252
Electrolytes......Page 260
Electrophoretic NMR......Page 268
Agriculture and Soils......Page 278
Coal Structure from Solid State NMR......Page 283
Fossil Fuels......Page 293
Aluminum-27 NMR of Solutions......Page 311
Boron NMR......Page 320
Ceramics......Page 334
Chiral Discrimination Using Chiral Ordering Agents......Page 338
Diamond Thin Films......Page 347
Diffusion in Solids......Page 354
Fluorine-19 NMR......Page 370
Germanium, Tin, and Lead NMR......Page 379
Hydrogen Molecules......Page 388
Hydrogen–Metal Systems......Page 397
Inorganic Chemistry Applications......Page 407
Inorganic Nuclei -Low Sensitivity Transition Metals......Page 418
Inorganic Solids......Page 428
Intercalation Compounds......Page 439
Lithium NMR......Page 448
Metallodrugs......Page 469
Microporous Materials and Xenon-129 NMR......Page 484
Molecular Sieves- Crystalline Systems......Page 491
Nitrogen NMR......Page 508
Noble Gas Elements......Page 538
Oxygen-17 NMR......Page 549
Phase Transitions and Critical Phenomena in Solids......Page 560
Phosphorus-31 NMR......Page 569
Polymorphism and Related Phenomena......Page 576
Quadrupolar Nuclei in Solids......Page 582
Quadrupolar Transition Metal and Lanthanide Nuclei......Page 603
Reactions in Zeolites......Page 614
Silica Surfaces- Characterization......Page 621
Silicon-29 NMR of Solid Silicates......Page 637
Silicon-29 NMR......Page 647
Sodium-23 NMR......Page 659
Steady-State Techniques for Low Sensitivity and Slowly Relaxing Nuclei......Page 666
Sulfur, Selenium, and Tellurium NMR......Page 674
Thallium NMR......Page 688
Tritium NMR......Page 696
Vanadium Catalysts- Solid State NMR......Page 708
Adsorbed Species -Spectroscopy and Dynamics......Page 721
Amphiphilic Liquid Crystalline Samples -Nuclear Spin Relaxation......Page 727
Centerband-Only Detection of Exchange (CODEX)-Efficient NMR Analysis of Slow Motions in Solids......Page 735
Deuteron Relaxation Rates in Liquid Crystalline Samples- Experimental Methods......Page 745
Liquid Crystalline Samples-Deuterium NMR......Page 756
Liquid Crystalline Samples-Relaxation Mechanisms......Page 765
Relaxation of Quadrupolar Nuclei Measured via Multiple Quantum Filtration......Page 771
Supercritical Fluids......Page 778
Amino Acids, Peptides and Proteins: Chemical Shifts......Page 789
Bacteriorhodopsin and Rhodopsin......Page 794
Biological Macromolecules......Page 804
Calmodulin......Page 825
Carbohydrates and Glycoconjugates......Page 832
Cobalt(II)- and Nickel(II)-Substituted Proteins......Page 863
Copper Proteins......Page 871
Natural Products......Page 878
Nitrogen-15 Chemical Shift Tensors and Organic Structure......Page 887
Oxygen-17 NMR- Applications in Biochemistry......Page 895
Structural Analysis Enhancements for Natural Products......Page 898
Vitamin B12......Page 907
Accuracy Limitations on Internuclear Distances Measured by REDOR......Page 912
Chemical Shift Tensors in Single Crystals......Page 921
Geometric Phases......Page 929
Homonuclear Recoupling Schemes in MAS NMR......Page 934
Multiple Quantum Coherences in Extended Dipolar Coupled Spin Networks......Page 939
Polymorphism and Related Phenomena......Page 949
REDOR and TEDOR......Page 955
Three-dimensional Molecular Structures in Uniformly Labelled Solids Determined Using Rotational Resonance in the Tilted Rotating Frame......Page 962
Carbanion Chemistry......Page 973
Carbon-13 Relaxation Measurements -Organic Chemistry Applications......Page 990
Carbon-13 Studies of Deuterium Labeled Compounds......Page 1000
Combinatorial Chemistry......Page 1005
Coupling Through Space in Organic Chemistry......Page 1011
Dynamics in Solid Organic Compounds-Intramolecular Motions......Page 1021
Fluorine-19 NMR of Solids Containing Both Fluorine and Hydrogen......Page 1030
Fluorine-19 NMR......Page 1050
Fullerenes and Related Molecules as Studied by Solid State NMR......Page 1059
Heterocycles......Page 1067
Hydrogen Bonding......Page 1073
Inclusion Compounds......Page 1079
Indirect Coupling Theory and Applications in Organic Chemistry......Page 1092
Intercalation Compounds......Page 1105
Isotope Effects in Carbocation Chemistry......Page 1114
Nitrogen NMR......Page 1119
Nitrogen-15 Chemical Shift Tensors and Organic Structure......Page 1149
Organic Chemistry Applications......Page 1157
Oxygen-17 NMR......Page 1172
Phosphorus-31 NMR......Page 1183
Polymorphism and Related Phenomena......Page 1190
Spectral Editing Techniques- Hydrocarbon Solids......Page 1196
Stereochemistry and Long Range Coupling Constants......Page 1203
Supramolecular Chemistry......Page 1213
Thioredoxin and Glutaredoxin......Page 1224
Tritium NMR......Page 1231
Vicinal 1H,1H Coupling Constants in Cyclic π-Systems......Page 1243
Amorphous Materials......Page 1246
Amorphous Silicon Alloys......Page 1270
Colloidal Systems......Page 1281
Ceramics......Page 1288
Ceramics Imaging......Page 1292
Agriculture and Soils......Page 1297
Coal Structure from Solid State NMR......Page 1302
Fossil Fuels......Page 1312
Geological Applications......Page 1330
Oil Reservoir Rocks Examined by MRI......Page 1339
Terrestrial Magnetic Field NMR......Page 1351
Well Logging......Page 1357
Ferroelectrics and Proton Glasses......Page 1367
Oxygen-17 NMR......Page 1381
Polymer Conformations in Glassy Solutions as Studied by Off-resonance Radiation......Page 1392
Quadrupolar Nuclei in Glasses......Page 1401
Amphiphilic Liquid- Crystalline Samples Nuclear Spin Relaxation......Page 1412
Anisotropy of Shielding and Coupling in Liquid Crystalline Solutions......Page 1420
Deuteron Relaxation Rates in Liquid Crystalline Samples- Experimental Methods......Page 1430
Dynamic NMR in Liquid Crystalline Solvents......Page 1441
Liquid Crystalline Samples Carbon-13 NMR......Page 1456
Liquid Crystalline Samples-Application to Macromolecular Structure Determination......Page 1464
Liquid Crystalline Samples-Chiral Smectic Phases......Page 1476
Liquid Crystalline Samples-Deuterium NMR......Page 1484
Liquid Crystalline Samples-Diffusion......Page 1493
Liquid Crystalline Samples-Relaxation Mechanisms......Page 1502
Liquid Crystalline Samples-Spectral Analysis......Page 1508
Liquid Crystalline Samples-Structure of Nonrigid Molecules......Page 1515
Liquid Crystals- General Considerations......Page 1522
Liquid Crystals- Mixed Magnetic Susceptibility Solvents......Page 1535
Local Field Experiments in Liquid Crystals......Page 1541
Lyotropic Liquid Crystalline Samples......Page 1548
Micellar Solutions and Microemulsions......Page 1556
Multiple Quantum Spectroscopy in Liquid Crystalline Solvents......Page 1568
Polymer Dispersed Liquid Crystals......Page 1577
Spinning Liquid Crystalline Samples......Page 1583
Structure of Rigid Molecules Dissolved in Liquid Crystalline Solvents......Page 1591
Two-Dimensional NMR of Molecules Oriented in Liquid Crystalline Phases......Page 1603
Chemical Exchange on Solid Metal Surfaces......Page 1613
Micellar Solutions and Microemulsions......Page 1618
Conducting Polymers......Page 1630
Coupled Spin Relaxation in Polymers......Page 1635
Polymer Blends- Miscibility Studies......Page 1642
Polymer Conformations in Glassy Solutions as Studied by Off-resonance Radiation......Page 1651
Polymer Dynamics and Order from Multidimensional Solid State NMR......Page 1660
Polymer Physics......Page 1675
Polymer Reactions......Page 1689
Polymerization and Statistical Models......Page 1697
Polymers- Regio-Irregular Structure......Page 1706
Polymers- Relaxation and Dynamics of Synthetic Polymers in Solution......Page 1712
Polymers Under Mechanical Tension......Page 1719
Polysaccharide Solid State NMR......Page 1730
Polysaccharides and Complex Oligosaccharides......Page 1736
Solid Biopolymers......Page 1742
Solid Polymers- Shielding and Electronic States......Page 1752
Structural and Dynamic Characterization of Soft Polymers by Solid State NMR and Field Gradient NMR......Page 1759
Incommensurate Systems......Page 1777
Quasicrystalline Compounds- Metallic Glasses......Page 1789
Ferroelectrics and Proton Glasses......Page 1797
Nuclear Ferromagnetism and Antiferromagnetism......Page 1811
Fast Ion Conductors......Page 1818
Hydrogen–Metal Systems......Page 1824
Knight Shift......Page 1834
Metallic Superconductors......Page 1841
Metals- Pure and Alloyed......Page 1851
Geometric Phases......Page 1859
Molten Salts......Page 1864
Nuclear Spin Superradiance......Page 1868
Ortho –Para Hydrogen at Low Temperature......Page 1883
Optically Pumped NMR of Semiconductors and Two-Dimensional Electron Systems......Page 1889
Quantum Tunneling Spectroscopy......Page 1897
Ruby NMR Laser......Page 1901
Liquid-state Quantum Computing......Page 1908
Quantum Exchange......Page 1918
Quantum Tunneling Spectroscopy......Page 1927
High Temperature Superconductors......Page 1931
Metallic Superconductors......Page 1943
Adsorbed Species -Spectroscopy and Dynamics......Page 1953
Chemical Exchange on Solid Metal Surfaces......Page 1959
Diamond Thin Films......Page 1964
Hydrogen–Metal Systems......Page 1971
Silica Surfaces- Characterization......Page 1981
Structure and Dynamics of Proteins Adsorbed at Biomaterial Interfaces......Page 1997
Accuracy Limitations on Internuclear Distances Measured by REDOR......Page 2008
Bacteriorhodopsin and Rhodopsin......Page 2017
Biological Systems Spin-3-2 Nuclei......Page 2027
Double-quantum Filtered NMR of Ordered Biological Tissues......Page 2039
Filamentous Bacteriophage Coat Protein......Page 2050
Glycolipids......Page 2055
Gramicidin Channels-Orientational Constraints for Defining High-Resolution Structures......Page 2063
Lipid Polymorphism......Page 2067
Membrane Proteins......Page 2073
Multiple-Resonance Multi-Dimensional Solid-State NMR of Proteins......Page 2082
Phospholipid–Cholesterol Bilayers......Page 2091
Polysaccharide Solid State NMR......Page 2098
Proton Chemical Shift Measurements in Biological Solids......Page 2104
Rotational Resonance in Biology......Page 2109
Solid Biopolymers......Page 2114
Structure and Dynamics of Proteins Adsorbed at Biomaterial Interfaces......Page 2124
Structure Determination of Solid Proteins Using MAS and Isotopic Enrichment......Page 2135
Structures of Larger Proteins, Protein–Ligand,and Protein–DNA Complexes by Multidimensional Heteronuclear NMR......Page 2143
Calmodulin......Page 2164
Chemical Exchange Effects in Biological Macromolecules......Page 2171
Diffusion-Based Studies of Aggregation, Binding and Conformation of Biomolecules Theory and Practice......Page 2181
Dynamics of Water in Biological Systems-Inferences from Relaxometry......Page 2192
Hydrogen Exchange and Macromolecular Dynamics......Page 2203
Oxygen-17 NMR- Applications in Biochemistry......Page 2209
Pancreatic Trypsin Inhibitor......Page 2212
Phage Lysozyme- Dynamics and Folding Pathway......Page 2220
Protein Dynamics from NMR Relaxation......Page 2225
Relaxation Effects Involving Cross Correlation in Biomolecules......Page 2231
Selective Relaxation Techniques in Biological NMR......Page 2241
Slow and Ultraslow Motions in Biology......Page 2251
Structure and Dynamics of Disordered Proteins......Page 2260
Amino Acids, Peptides and Proteins Chemical Shifts......Page 2269
Bilayer Membranes Deuterium and Carbon-13 NMR......Page 2274
Bilayer Membranes Proton and Fluorine-19 NMR......Page 2289
Chemical Exchange Effects in Biological Macromolecules......Page 2299
Membranes- Carbon-13 NMR......Page 2309
Membranes- Deuterium NMR......Page 2315
Membranes- Phosphorus-31 NMR......Page 2322
Nucleic Acid Flexibility and Dynamics- Deuterium NMR......Page 2329
Phospholipid–Cholesterol Bilayers......Page 2335
Protein Dynamics from Solid State NMR......Page 2342
Selective Relaxation Techniques in Biological NMR......Page 2347
Slow and Ultraslow Motions in Biology......Page 2357
Bacterial Chemotaxis Proteins Fluorine-19 NMR......Page 2366
Biological Macromolecules......Page 2373
Biological Macromolecules-Structure Determination in Solution......Page 2394
Cadmium-113 NMR- A Surrogate Probe for Zinc and Calcium in Proteins......Page 2402
Calcium-Binding Proteins......Page 2409
Calmodulin......Page 2417
Carbohydrates and Glycoconjugates......Page 2424
Carbon and Nitrogen Chemical Shifts of Solid State Enzymes......Page 2455
Carbonic Anhydrase......Page 2466
Cell Suspensions......Page 2470
DNA Triplexes,Quadruplexes, and Aptamers......Page 2482
DNA-A-, B-, and Z-......Page 2488
DNA–Cation Interactions-Quadrupolar Studies......Page 2495
Drug–Nucleic Acid Interactions......Page 2504
Half-Filter Experiments-Proton–Carbon-13......Page 2514
Haptens and Antibodies......Page 2519
Homonuclear Three-Dimensional NMR of Biomolecules......Page 2526
Lipoproteins......Page 2541
Liquid Crystalline Samples-Application to Macromolecular Structure Determination......Page 2550
Membrane Lipids of Acholeplasma laidlawii......Page 2562
Membrane Proteins......Page 2568
Metallothioneins......Page 2577
Molecular Motions- T1 Frequency Dispersion in Biological Systems......Page 2584
Muscle Proteins......Page 2590
Nucleic Acid Structures in Solution- Sequence Dependence......Page 2602
Nucleic Acids- Base Stacking and Base Pairing Interactions......Page 2614
Nucleic Acids- Phosphorus-31 NMR......Page 2618
Nucleic Acids- Spectra, Structures, and Dynamics......Page 2625
Oxygen-18 in Biological NMR......Page 2639
Pancreatic Trypsin Inhibitor......Page 2644
Peptide and Protein Secondary Structural Elements......Page 2652
Peptide Hormones......Page 2661
Peptides and Polypeptides......Page 2667
Polysaccharides and Complex Oligosaccharides......Page 2678
Protein Hydration......Page 2684
Protein Modules......Page 2689
Proteins and Protein Fragments- Folding......Page 2695
Ribosomal RNA......Page 2705
RNA Structure and Function- Modified Nucleosides......Page 2710
Saccharide-Protein Interactions......Page 2717
SH2 Domain Structures......Page 2725
Sonicated Membrane Vesicles......Page 2731
Structures of Larger Proteins, Protein–Ligand,and Protein–DNA Complexes by Multidimensional Heteronuclear NMR......Page 2738
Synthetic Peptides......Page 2759
Thioredoxin and Glutaredoxin......Page 2768
Transverse Relaxation-optimized NMR Spectroscopy with Biomacromolecular Structures in Solution......Page 2775
Biosynthesis and Metabolic Pathways Carbon-13 and Nitrogen-15 NMR......Page 2784
Biosynthesis and Metabolic Pathways Deuterium NMR......Page 2789
Biological Macromolecules- NMR Parameters......Page 2793
Chemical Shifts in Biochemical Systems......Page 2805
Nucleic Acids- Chemical Shifts......Page 2812
Oxygen-17 NMR- Applications in Biochemistry......Page 2816
Vicinal Coupling Constants and Conformation of Biomolecules......Page 2819
Protein Structures- Relaxation Matrix Refinement......Page 2833
Relaxation Matrix Refinement of Nucleic Acids......Page 2844
D-Lactate Dehydrogenase......Page 2850
Enzymatic Transformations Isotope Probes......Page 2857
Enzyme-Catalyzed Exchange Magnetization Transfer Measurements......Page 2865
Motional Effects on Protein Structure- Acyl Carriers......Page 2872
Proteases......Page 2876
Time-Resolved Solid State NMR of Enzyme–Substrate Interactions......Page 2884
Dietary Changes Studied by MRS......Page 2891
Foods and Grains Studied by MRS and MRI......Page 2897
Cobalt(II)- and Nickel(II)-Substituted Proteins......Page 2900
Copper Proteins......Page 2908
Distance Geometry......Page 2915
Enzymes Utilizing ATP-Kinases, ATPases and Polymerases......Page 2925
Heme Peroxidases......Page 2934
Hemoglobin......Page 2941
Iron–Sulfur Proteins......Page 2951
Metallodrugs......Page 2956
Mitochondrial Cytochrome c......Page 2971
Myoglobin......Page 2975
Nonheme Iron Proteins......Page 2979
Transferrins......Page 2992
Zinc Fingers......Page 3001
Tritium NMR in Biology......Page 3010
Water Signal Suppression in NMR of Biomolecules......Page 3019
Plant Physiology......Page 3031
Wood and Wood Chars......Page 3037
Anisotropically Restricted Diffusion in MRI......Page 3042
Brain Parenchyma Motion Observed by MRI......Page 3047
Diffusion and Perfusion in MRI......Page 3056
Diffusion- Clinical Utility of MRI Studies......Page 3068
Methods and Applications of Diffusion MRI......Page 3078
Brain MRS of Human Subjects......Page 3097
Brain- Sensory Activation Monitored by Induced Hemodynamic Changes with Echo Planar MRI......Page 3105
Fluorine-19 MRS -General Overview and Anesthesia......Page 3110
Functional MRI at High Fields-Practice and Utility......Page 3122
Functional MRI -Theory and Practice......Page 3142
Functional Neuroimaging Artifacts......Page 3149
Hemodynamic Changes Owing to Sensory Activation of the Brain Monitored by Echo-Plana Imaging......Page 3158
Postoperative Trauma Observed by MRI......Page 3164
Abdominal MRA......Page 3167
Assessment of Regional Blood Flow and Volume by Kinetic Analysis of Contrast-Dilution Curves......Page 3174
Cerebral Perfusion Imaging by Exogenous Contrast Agents......Page 3178
CSF Velocity Imaging......Page 3191
Head and Neck Studies Using MRA......Page 3199
Peripheral Vasculature MRA......Page 3209
Phase Contrast MRA......Page 3217
Time-of-Flight Method of MRA......Page 3232
Whole Body Magnetic Resonance Angiography......Page 3237
Blood Flow - Quantitative Measurement by MRI......Page 3249
Breast MRI......Page 3264
Cardiac Gating Practice......Page 3270
Cardiovascular NMR to Study Function......Page 3276
Coronary Artery Disease Evaluated by MRI......Page 3284
Heart -Clinical Applications of MRI......Page 3288
Lung and Mediastinum MRI......Page 3299
Marker Grids for Observing Motion in MRI......Page 3308
NMR Spectroscopy of the Human Heart......Page 3313
Brain Infection and Degenerative Disease Studied by Proton MRS......Page 3323
Brain MRS of Infants and Children......Page 3331
Central Nervous System Degenerative Disease Observed by MRI......Page 3346
Cranial Nerves Investigated by MRI......Page 3352
Degenerative Disk Disease Studied by MRI......Page 3379
Eye, Orbit, Ear, Nose, and Throat Studies Using MRI......Page 3389
Head and Neck Investigations by MRI......Page 3402
Hemorrhage in the Brain and Neck Observed by MRI......Page 3411
Intracranial Infections......Page 3417
Ischemic Stroke......Page 3426
Magnetic Resonance Imaging of White Matter Disease......Page 3438
MRI and MRS of Neuropsychiatry......Page 3452
Pediatric Brain MRI- Applications in Neonates and Infants......Page 3461
Pituitary Gland and Parasellar Region Studied by MRI......Page 3475
Sodium-23 Magnetic Resonance of Human Subjects......Page 3483
Structural and Functional MR in Epilepsy......Page 3490
Systemically Induced Encephalopathies- Newer Clinical Applications of MRS......Page 3500
Temporomandibular Joint MRI......Page 3518
Applications of 19F-NMR to Oncology......Page 3523
Brain Neoplasms in Humans Studied by Phosphorus-31 NMR Spectroscopy......Page 3528
Brain Neoplasms Studied by MRI......Page 3536
Body Fat Metabolism-Observation by MR Imaging and Spectroscopy......Page 3541
Dietary Changes Studied by MRS......Page 3549
Hepatic and Other Systemically Induced Encephalopathies-Applications of MRS......Page 3555
In Vivo Hepatic MRS of Humans......Page 3563
Kidney, Prostate, Testicle, and Uterus of Subjects Studied by MRS......Page 3575
Liver, Pancreas, Spleen,and Kidney MRI......Page 3584
Male Pelvis Studies Using MRI......Page 3591
MRI of the Female Pelvis......Page 3600
Pediatric Body MRI......Page 3611
Tissue Behavior Measurements Using Phosphorus-31 NMR......Page 3619
Imaging and Spectroscopy of Muscle......Page 3626
Imaging of Trabecular Bone......Page 3636
MRI of Musculoskeletal Neoplasms......Page 3649
Peripheral Joint Magnetic Resonance Imaging......Page 3658
Peripheral Muscle Metabolism Studied by MRS......Page 3666
Skeletal Muscle Evaluated by MRI......Page 3676
High-Field Whole Body Systems......Page 3682
Low-Field Whole Body Systems......Page 3690
Magnetic Resonance Imaging- A Historical Overview......Page 3700
MRI at Midfield Strength......Page 3711
MRI in Clinical Medicine......Page 3719
Sensitivity of Whole Body MRI Experiments......Page 3728
Whole Body MRI- Strategies Designed to Improve Patient Throughput......Page 3737
Whole Body Studies- Impact of MRS......Page 3746
Gastroscopy and Colonoscopy......Page 3756
Interventional MRI-Specialist Facilities and Techniques......Page 3764
MR-Guided Biopsy, Aspiration, and Cyst Drainage......Page 3774
MR-Guided Therapy in the Brain......Page 3784
Neurosurgical Procedures Monitored by Intraoperative MRI......Page 3793
Temperature Measurement In Vivo Using NMR......Page 3805
Therapy Monitoring by MRI......Page 3813
Thermal Therapies in the Body Monitored by MRI......Page 3819
Dynamic Nuclear Polarization and High-Resolution NMR of Solids......Page 3827
Electron–Nuclear Hyperfine Interactions......Page 3837
Electron–Nuclear Interactions......Page 3842
Electron–Nuclear Multiple Resonance Spectroscopy......Page 3859
EPR and In Vivo EPR-Roles for Experimental and Clinical NMR Studies......Page 3876
In Vivo ESR Imaging of Animals......Page 3887
Accuracy Limitations on Internuclear Distances Measured by REDOR......Page 3892
Dipolar and Indirect Coupling Tensors in Solids......Page 3901
Distance Geometry......Page 3912
Magic Angle Spinning Carbon-13 Lineshapes-Effect of Nitrogen-14......Page 3922
Magic Angle Spinning-Effects of Quadrupolar Nuclei on Spin-1-2 Spectra......Page 3930
Magnetic Field Induced Alignment of Molecules......Page 3936
Multiple Quantum Coherence in Spin-1-2 Dipolar Coupled Solids......Page 3942
Multiple Quantum Coherences in Extended Dipolar Coupled Spin Networks......Page 3953
Multiple Quantum NMR in Solids......Page 3963
Multiple-quantum Magic-angle Spinning Experiments on Half-integer Nuclei-Fundamentals......Page 3973
REDOR and TEDOR......Page 3986
Spin Diffusion in Solids......Page 3993
Three-dimensional Molecular Structures in Uniformly Labelled Solids Determined Using Rotational Resonance in the Tilted Rotating Frame......Page 4000
Anisotropy of Shielding and Coupling in Liquid Crystalline Solutions......Page 4011
Coupling Through Space in Organic Chemistry......Page 4021
Dipolar and Indirect Coupling Tensors in Solids......Page 4031
Indirect Coupling Theory and Applications in Organic Chemistry......Page 4042
Indirect Coupling-Intermolecular and Solvent Effects......Page 4055
Indirect Coupling-Semiempirical Calculations......Page 4059
Indirect Nuclear Spin–Spin Coupling Tensors......Page 4064
Isotope Effects on Chemical Shifts and Coupling Constants......Page 4073
Quantum Exchange......Page 4090
Relativistic Computation of NMR Shieldings and Spin–Spin Coupling Constants......Page 4099
Relaxation of Transverse Magnetization for Coupled Spins......Page 4117
Relaxation Processes in Coupled-Spin Systems......Page 4123
Stereochemistry and Long Range Coupling Constants......Page 4143
Through-Bond Experiments in Solids......Page 4153
Vicinal 1H,1H Coupling Constants in Cyclic π-Systems......Page 4169
Vicinal Coupling Constants and Conformation of Biomolecules......Page 4172
Cryogenic NMR Probes-Applications......Page 4186
Field Gradients and Their Application......Page 4189
Instrumentation for the Home Builder......Page 4205
Microprobes and Methodologies for Spectral Assignments- Applications......Page 4212
Probe Design and Construction......Page 4226
Probes for High Resolution......Page 4236
Probes for Special Purposes......Page 4242
Rapid Scan Correlation Spectroscopy......Page 4246
Sensitivity of the NMR Experiment......Page 4252
Shimming of Superconducting Magnets......Page 4263
Solid State Probe Design......Page 4280
Spectrometers- A General Overview......Page 4291
SQUIDs......Page 4305
Knight Shift......Page 4309
Metals- Pure and Alloyed......Page 4316
Paramagnetic Relaxation in Solution......Page 4324
Quasicrystalline Compounds- Metallic Glasses......Page 4331
High Speed MAS of Half-Integer Quadrupolar Nuclei in Solids......Page 4339
Magic Angle Spinning Carbon-13 Lineshapes-Effect of Nitrogen-14......Page 4348
Magic Angle Spinning-Effects of Quadrupolar Nuclei on Spin-1-2 Spectra......Page 4356
Magnetic Field Induced Alignment of Molecules......Page 4362
MQMAS Advances......Page 4368
Nutation Spectroscopy of Quadrupolar Nuclei......Page 4394
Overtone Spectroscopy of Quadrupolar Nuclei......Page 4399
Quadrupolar Interactions......Page 4404
Quadrupolar Nuclei in Glasses......Page 4414
Quadrupolar Nuclei in Liquid Samples......Page 4425
Relaxation Theory for Quadrupolar Nuclei......Page 4436
Satellite Transition NMR Spectroscopy of Half-Integer Quadrupolar Nuclei under Magic-Angle Spinning......Page 4445
Concentrated Solution Effects......Page 4455
Dipolar Field and Radiation Damping-Collective Effects in Liquid-state NMR......Page 4462
Brownian Motion and Correlation Times......Page 4499
Liouville Equation of Motion......Page 4516
Nuclear Overhauser Effect......Page 4530
Relaxation- An Introduction......Page 4542
Relaxation Effects Involving Cross Correlation in Biomolecules......Page 4557
Relaxation Effects of Chemical Exchange......Page 4567
Relaxation Mechanisms-Magnetization Modes......Page 4578
Relaxation of Coupled Spins from Rotational Diffusion......Page 4586
Relaxation of Quadrupolar Nuclei Measured via Multiple Quantum Filtration......Page 4602
Relaxation of Transverse Magnetization for Coupled Spins......Page 4609
Relaxation Processes- Cross Correlation and Interference Terms......Page 4615
Relaxation Processes in Coupled-Spin Systems......Page 4622
Relaxation Theory -Density Matrix Formulation......Page 4642
Relaxation Theory for Quadrupolar Nuclei......Page 4650
Rotating Frame Spin–Lattice Relaxation Off-Resonance......Page 4659
Spin–Rotation Relaxation Theory......Page 4667
Ultraslow Motions in Solids......Page 4672
Accurate Determination of Nuclear Quadrupole Coupling Constants and other NMR Parameters in Liquids from the Combination of Molecular Dynamics Simulations and ab initio Calculations......Page 4680
Anisotropy of Shielding and Coupling in Liquid Crystalline Solutions......Page 4692
Chemical Shift Scales on an Absolute Basis......Page 4702
Chemical Shift Tensor Measurement in Solids......Page 4711
Chemical Shift Tensors in Single Crystals......Page 4727
Chemical Shift Tensors......Page 4735
Chemical Shifts in Biochemical Systems......Page 4760
Electric Field Effects on Shielding Constants......Page 4767
Isotope Effects on Chemical Shifts and Coupling Constants......Page 4778
Magnetic Susceptibility and High Resolution NMR of Liquids and Solids......Page 4795
Nitrogen-15 Chemical Shift Tensors and Organic Structure......Page 4804
Nucleic Acids- Chemical Shifts......Page 4812
Relativistic Computation of NMR Shieldings and Spin–Spin Coupling Constants......Page 4816
Semiempirical Chemical Shift Calculations......Page 4834
Shielding Calculations- IGLO Method......Page 4844
Shielding Calculations- LORG and SOLO Approaches......Page 4852
Shielding Calculations- Perturbation Methods......Page 4860
Shielding Calculations......Page 4868
Shielding in Small Molecules......Page 4878
Shielding- Overview of Theoretical Methods......Page 4887
Shielding Tensor Calculations......Page 4898
Shielding Theory- GIAO Method......Page 4905
Solid Polymers- Shielding and Electronic States......Page 4911
Analysis of High-Resolution Solution State Spectra......Page 4918
Analysis of Spectra-Automatic Methods......Page 4937
Carbon-13 Spectral Simulation......Page 4943
Chemical Shift Scales on an Absolute Basis......Page 4954
Computer Assisted Structure Elucidation......Page 4963
Data Processing......Page 4969
Diffusion-Ordered Spectroscopy (DOSY)......Page 4980
Fourier Transform and Linear Prediction Methods......Page 4989
Fourier Transform Spectroscopy......Page 4997
Heteronuclear Assignment Techniques......Page 5008
Liouville Equation of Motion......Page 5017
Liquid Crystalline Samples-Spectral Analysis......Page 5031
Magic Angle Spinning Carbon-13 Lineshapes-Effect of Nitrogen-14......Page 5038
Magic Angle Spinning-Effects of Quadrupolar Nuclei on Spin-1-2 Spectra......Page 5046
Magnetic Equivalence......Page 5052
Maximum Entropy Reconstruction......Page 5063
Microprobes and Methodologies for Spectral Assignments- Applications......Page 5072
Multiple Quantum Spectroscopy in Liquid Crystalline Solvents......Page 5086
Proton Chemical Shift Measurements in Biological Solids......Page 5095
Reference Deconvolution......Page 5100
Sideband Analysis in Magic Angle Spinning NMR of Solids......Page 5107
Spectral Editing Techniques- Hydrocarbon Solids......Page 5115
Spinning Sideband Analysis for Spin-1-2 Nuclei......Page 5122
Average Hamiltonian Theory......Page 5132
Cross Polarization in Rotating Solids- Spin-1,2 Nuclei......Page 5139
Cross Polarization in Solids......Page 5145
Dipolar Spectroscopy- Transient Nutations and Other Techniques......Page 5153
Double Quantum Coherence......Page 5159
Double-Quantum NMR Spectroscopy of Dipolar Coupled Spins Under Fast Magic-Angle Spinning......Page 5168
Dynamic Frequency Shift......Page 5183
Dynamic Spin Ordering of Matrix Isolated Methyl Rotors......Page 5191
Echoes in Solids......Page 5204
Electron–Nuclear Hyperfine Interactions......Page 5210
Electron–Nuclear Interactions......Page 5215
Electron–Nuclear Multiple Resonance Spectroscopy......Page 5232
Floquet Theory......Page 5249
Internal Spin Interactions and Rotations in Solids......Page 5265
Liouville Equation of Motion......Page 5283
Low Spin Temperature NMR......Page 5297
Maximum Entropy Reconstruction......Page 5307
Multiple Quantum Coherences in Extended Dipolar Coupled Spin Networks......Page 5316
Multiple Quantum NMR in Solids......Page 5326
Nuclear Spin Properties and Conventions for Chemical Shifts (IUPAC Recommendations 2001†)......Page 5336
Probe Design and Construction......Page 5351
Quantum Exchange......Page 5361
Quantum Optics- Concepts of NMR......Page 5370
Radiofrequency Pulses- Response of Nuclear Spins......Page 5378
Relaxation Theory -Density Matrix Formulation......Page 5384
Rotating Solids......Page 5392
Rudimentary NMR-The Classical Picture......Page 5403
Solid State Probe Design......Page 5411
Thermodynamics of Nuclear Magnetic Ordering......Page 5422
Abragam, Anatole: ‘The Bible’......Page 5429
Abraham, Raymond J.: A Brief History of Proton Chemical Shifts......Page 5431
Ackerman, Joseph J. H.:Oxford Knights......Page 5433
Ailion, David C.: The First Observations of Ultraslow Motions......Page 5435
Aime, Silvio: A Taste of NMR in Inorganic Chemistry......Page 5437
Anderson, Weston A.: Early NMR Experiences and Experiments......Page 5438
Ando, Isao: Structures and Electronic States of Polymers as Studied by High-Resolution NMR Spectroscopy Combined with Quantum Chemistry......Page 5447
Andrew, E. Raymond:Spinning the Spins: A Lifetime in NMR......Page 5452
Anet, Frank A. L.: A Lapsed Organic Chemist in the Wonderland of NMR......Page 5459
Arata, Yoji: Early Days of NMR in Japan......Page 5463
Arnold, James T.: Early Perceptions in Nuclear Magnetic Resonance (NMR)......Page 5465
Bain, Alex D.: Early Development of Homonuclear 2D NMR (From the Outside)......Page 5472
Balaban, Robert S.:Personal Perspective on the History of NMR......Page 5473
Barfield, Michael:Thirty-Three Years of NMR Parameters......Page 5475
Bax, Ad: NMR of Ethanol and Interferon-γ......Page 5477
Becker, Edwin D.: NMR at the NIH: Inception and Growth Over Four Decades......Page 5483
B´en´e, Georges-J.: The Early Days of NMR Research in Geneva......Page 5487
Bertini, Ivano: A Life with Paramagnetic Molecules......Page 5489
Bible, Roy H. Jr.: NMR:An Organic Chemist’s Dream Come True......Page 5491
Blinc, Robert: The AMPERE Society and the Development of Magnetic Resonance in Eastern Europe......Page 5493
Bloch, Felix: The Principle of Nuclear Induction......Page 5494
Bloembergen, Nicolaas: My Early Years in NMR,1946–48......Page 5500
Bloom, Myer: Personal Views of NMR History......Page 5505
Bodenhausen, Geoffrey:Traveling through the World of Magnetic Resonance in the 1970s......Page 5512
Bothner-By, Aksel A.:Computer Analysis of High-Resolution NMR Spectra......Page 5515
Bottomley, Paul A.: The Development of High-Field NMR Imaging: 0.12T to 1.5T......Page 5519
Bovey, Frank A.: NMR of Polymers......Page 5522
Brey, Wallace S.: The First 40 Years Should Be the Hardest......Page 5526
Budinger, Thomas F.:Perspectives on Reconstruction Tomography and Magnetic Field Physiological Effects......Page 5529
Bydder, Graeme M.:Magnetic Resonance at Hammersmith Hospital......Page 5530
Callaghan, Paul T.: From γ -Rays to Gradients......Page 5535
Carr, Herman Y.: Early Years of Free Precession Revisited......Page 5537
Clough, Stanley: NMR and Quantum Tunneling Rotation......Page 5545
Codrington, Robert S.: Comments on NMR Instrument Development......Page 5547
Cohen, Jack S.:Recollections of Early NMR Applications to Proteins and Cells......Page 5548
Mildred Cohn:Peregrinations of an Enzymologist in NMR......Page 5550
Corio, Paul L.:High-Resolution NMR at Columbia University......Page 5553
Cotts, Robert M.: Historical Recollections......Page 5555
Crooks, Lawrence E.: Field Strength Selection for MR Imaging......Page 5557
Dadok, Josef: High-Field NMR Instrumentation......Page 5559
Diehl, Peter: NMR at the Physics Department of the University of Basel, Switzerland (1949–96)......Page 5565
Doddrell, David M.: An Historical Perspective of Research Based Upon Misguided Advice......Page 5568
Doskocilov´a, Danica & Schneider, Bohdan: Development of Magic Angle Rotation for the Narrowing of Proton NMR Lines in Organic Materials......Page 5570
Doty, F. David: A Random Walk Toward High-Speed Sample Spinning......Page 5572
Dwek, Raymond A.: From Antibodies to Glycobiology......Page 5574
Dybowski, Cecil: Bob Vaughan and Solid State NMR at Caltech in the 1970s......Page 5576
Ellis, Paul D.: Multinuclear MR Experiments, the Surrogate Probe Strategy, and Other Fun & Games......Page 5578
Emsley, James W.: Having Fun with Liquid Crystals......Page 5580
Engelhardt, G¨ unter: Silicon-29 NMR of Silicates: From Liquids to Solids. An Historical Perspective......Page 5583
Ernst, Richard R.: The Success Story of Fourier Transformation in NMR......Page 5585
Farrar, Thomas C.: Historical Reminiscences of Some NMR Experiences......Page 5599
Feeney, James: Personal Reminiscences on NMR......Page 5602
Ferguson, Raymond C.:William D. Phillips and Nuclear Magnetic Resonance Spectroscopy at DuPont......Page 5604
Fiat Daniel: The International Society of Magnetic Resonance (ISMAR). Landmarks and Highlights......Page 5609
Fors´en, Sture: ‘Saturation Transfer’ and ‘TSI’—Early Days and Nights of NMR in Sweden......Page 5611
Fraenkel, Gideon:Reminiscence of NMR......Page 5613
Frahm, Jens: Toward Rapid NMR Imaging......Page 5614
Fraissard, J.: A Look at Solid Catalysts by NMR......Page 5619
Freeman, Ray: Double Resonance Methods in High-Resolution NMR......Page 5622
Fujiwara, Shizuo: Early Development of the Study of NMR in Japan......Page 5628
Gadian, David G.: From Brawn to Brain......Page 5630
Garroway, Allen N.:Origins of MRI—A Personal View......Page 5631
Gerstein, B. C.: The Vaughan Days, CRAMPS, and Transient Techniques in NMR......Page 5633
Goldman, Maurice: The Time when Spin Temperature was Hot Stuff......Page 5636
Gorenstein, David G.:Developments in 31P NMR......Page 5639
Govil, Girjesh: Nuclear Magnetic Resonance in India: A Historical Sketch......Page 5641
Grant, David M.:Carbon-13 Magnetic Resonance—An Exquisite NMR Garden of Surprises......Page 5642
Griffin, Robert G.:Perspectives of Magnetic Resonance......Page 5649
G¨unther, Harald: From Organic Chemistry to NMR—A Personal Experience of Magnetization Transfer......Page 5656
Gutowsky, Herbert S.: The Coupling of Chemical and Nuclear Magnetic Phenomena......Page 5659
Haeberlen, Ulrich: The Early Days of Multiple Pulse NMR......Page 5667
H¨agele, Gerhard: Analysis and Simulation of High-Resolution 1D NMR Spectra. Some Steps Closer to Automation......Page 5671
Hahn, Erwin L.: Pulsed NMR—A Personal History......Page 5673
Hall, Laurance D.: NMR Studies of Carbohydrates......Page 5679
Harris, Robin K.: Chemical Magnetic Resonance goes Multinuclear......Page 5683
Hennel, Jacek W.: Poland. Early NMR......Page 5687
Hinshaw, Waldo: Notes on the History of MR Imaging from my Perspective......Page 5689
Hoult, D. I.: Biomedical NMR Instrumentation—A Personal Viewpoint......Page 5694
Hurd, Ralph E.: A Brief History of Gradients in NMR......Page 5698
Hyde, James S.: The NMR/EPR Interface at Varian, ENDOR, and notes on Zavoisky......Page 5700
Jackman, Lloyd M.: NMR in Organic Chemistry–the Fabulous Fifties......Page 5702
Jakobsen, Hans J.: A Retrospect on the Development of High-Speed Sample Spinners for Solids since 1980......Page 5704
James, Thomas L.: Time for Preparation and Evolution. But what is the Mechanism for Relaxation?......Page 5706
Jameson, Cynthia J.: Early Work on the Ranges of Chemical Shifts and Signs of Coupling Constants......Page 5707
Jardetzky, Oleg: NMR in Molecular Biology—A History of Basic Ideas......Page 5709
Jeener, Jean: Reminiscences about the Early Days of 2D NMR......Page 5716
Johnson, Charles S. Jr.: The Evolution of Ideas about Optical Analogies to PFGNMR and the Visualization of PFGNMR Experiments......Page 5718
Johnson, LeRoy F.: My Early Days in NMR Spectroscopy......Page 5720
Jonas, Jiri: NMR and High Pressure......Page 5722
Kaplan, Jerome I.: Chemical Exchange in Various Guises......Page 5725
Kaptein, Robert: The Early Days of CIDNP......Page 5728
Karplus, Martin: Theory of Vicinal Coupling Constants......Page 5730
Keller, Tony: The Development of the First Multinuclear Fourier NMR Spectrometers......Page 5733
Kessler, Horst: Dynamics by NMR......Page 5735
Khetrapal, C. L.:Development of NMR of Oriented Systems......Page 5737
Klein, Melvin P.:Recollections of 40 Years of Magnetic Resonance at Berkeley......Page 5739
Klinowski, Jacek: Historical Sketch: Molecular Sieves......Page 5741
Knight, Walter D.: The Knight Shift......Page 5743
Kochelaev, Boris I.: Discovery of Electron Spin Resonance......Page 5747
Koenig, Seymour H.: I. I. Rabi, F. Bloch, E. M. Purcell, and the History of NMR and Relaxometry......Page 5750
Kowalewski, V. J.:Tribulations of a Young Physicist with a New Phenomenon......Page 5753
Kumar, Anil: Development of Two-Dimensional NMR—My Perception......Page 5754
La Mar, Gerd N.: NMR of Paramagnetic Proteins......Page 5756
Lambert, Joseph B.: The First Observation of Nitrogen-15 Nuclear Magnetic Resonances......Page 5758
Laszlo, Pierre: Getting Acquainted with a Spin-3/2 Nucleus......Page 5759
Lauterbur, Paul C.: One Path out of Many—How MRI Actually Began......Page 5761
Led, Jens J.: Aspects of NMR Studies of Paramagnetic Metal Complexes of Biological Relevance. A Historical Sketch......Page 5765
Lemieux, Raymond U.: First Observations: The Dependence on Torsion Angle of the Magnitude of the Coupling Constant for Vicinal Hydrogens and its Sign Compared to that for Geminal Hydrogens......Page 5768
Levitt, Malcolm H.: A Cyclic Evolution In Spin Cyclic Evolution In Spin......Page 5770
Levy, George C.:Recollections: Computers in the Early Days of 13C NMR and 25 Years of Growth in NMR Computing......Page 5772
L¨osche, Artur: The Beginnings of NMR in Leipzig......Page 5775
Lowe, Irving J.: My Life in the Rotating Frame......Page 5776
Lunazzi, Lodovico:Conformers and Enantiomers, Rotations and Stereomutations: an NMR Playground for an Organic Chemist......Page 5780
Lutz, Otto: Heteronuclear Magnetic Resonance......Page 5782
Luz, Zeev: The Early Days of NMR in Israel......Page 5784
Lynden-Bell, Ruth M.:Reminiscences of Early Days of NMR......Page 5790
Maciel, Gary E.: A Little Polarization Can be Good for You......Page 5792
Mansfield, Peter: A Personal View of My Involvement in the Development of NMR and the Conception and Development of MRI......Page 5799
Maraviglia, Bruno: A Personal Perspective about NMR Evolution......Page 5803
Margulis, Alexander R.:How NMR was Started at the University of California, San Francisco (UCSF)......Page 5805
Marshall, Alan G.: Ion Cyclotron Resonance Mass Spectrometry: a Brief History......Page 5807
Martin, G´erard J. Maryvonne L.: Ode to Ethanol......Page 5811
McConnell, Harden M.:Spin Chemistry......Page 5813
McDowell, Charles A.: Four Decades of Chemical NMR at the University of British Columbia (UBC)......Page 5815
McLauchlan, Keith A.:NMR Memories......Page 5817
Mehring, Michael: Advent and Evolution of High-Resolution NMR in Solids: A Personal View......Page 5819
Mildvan, Albert S.: Early Applications to Enzymes of Paramagnetic Effects on Nuclear Relaxation......Page 5821
Morris, Gareth A.: The Origins of DANTE......Page 5824
Nagayama, Kuniaki: The First Protein Two-Dimensional (2D) NMR......Page 5825
Nakanishi, Koji: First Encounter with NOE in Natural Products—the Ginkgolides......Page 5827
Norberg, Richard E.: NMR in Urbana and St. Louis......Page 5830
Oldfield, Eric: NMR Adventures in Chemistry and Biology......Page 5833
Opella, Stanley J.: NMR Spectroscopy and Structural Biology......Page 5835
Overhauser, Albert W.:Dynamic Nuclear Polarization......Page 5839
Packard, Martin E.:Nuclear Induction at Stanford and the Transition to Varian......Page 5843
Packer, Ken: Connections (or One Thing Leads to Another)......Page 5852
Pake, George E.: A Graduate Student and Young Faculty Physicist Wanders into NMR: 1946–53......Page 5854
Pfeifer, Harry: Leipzig, Summer 1951......Page 5858
Pines, Alexander: Solid State NMR: Some Personal Recollections......Page 5862
Poole, Charles P. Jr.: The Dance of the Nucleons......Page 5869
Pound, Robert V.: Early Days in NMR......Page 5871
Powles, Jack: Reminiscences of the Early Days of NMR......Page 5877
Proctor, Warren G.: When You and I Were Young, Magnet......Page 5879
Purcell, Edward M.:Research in Nuclear Magnetism......Page 5882
Radda, George K.: The Development of In Vivo NMR in Oxford......Page 5887
Radeglia, Reiner & Jancke, Harald: The History of the NMR Laboratory in the Former Central Institute for Physical Chemistry of the East German Academy of Sciences in Berlin......Page 5893
Ramsey, Norman F.:Origins of Magnetic Resonance......Page 5896
Randall, Edward W.:“Double, Double, Toil and Trouble” (Alias Double Resonance)......Page 5901
Raynes, W. T.: Early Work on Gas-Phase Chemical Shifts......Page 5903
Redfield, Alfred G.:Foundations and Structures......Page 5905
Reeves, Leonard W.: Early Application of NMR to Chemistry at the National Research Council of Canada......Page 5912
Richards, Rex:Development of NMR in Oxford......Page 5914
Rigden, John S.: Rabi’s Resonance Method......Page 5919
Roberts, John D.: A Personal NMR Odyssey......Page 5925
Rogers, Emery H.:Remembrance of NMR Things Past......Page 5934
Saika, A.: Early Applications of NMR in Chemistry and Theoretical Calculations of NMR Parameters Related to the Electronic Structure of Molecules......Page 5936
Samoson, Ago:Development of High-Resolution NMR of Quadrupole Nuclei in Solids......Page 5938
Sanders, Jeremy K. M.:Luck, Ignorance, and Daring in Research: NMR Spectroscopy of Nature’s Plastics and Spiders’ Webs......Page 5940
Saunders, Martin: The First NMR Spectrum of a Protein......Page 5942
Schaefer, Jacob: A Brief History of the Combination of Cross Polarization and Magic Angle Spinning......Page 5943
Schaefer, Ted: A Canadian Prairie Youth Discovers the Delights of NMR......Page 5950
Schneider, William G.:Early Research on High-Resolution Proton Magnetic Resonance......Page 5952
Scott, A. Ian: 13C NMR Studies of Biosynthesis. A Quarter Century in Retrospect......Page 5955
Seelig, Joachim: NMR and Membrane Structure......Page 5957
Sergeyev, Nickolai M.:Isotope Effects On Spin–Spin Coupling Constants......Page 5959
Shapiro, Bernard L.: The NMR Newsletter......Page 5962
Shaw, Derek: From 5-mm Tubes to Man. The Objects Studied by NMR Continue to Grow......Page 5964
Sheppard, Norman:NMR—Some Reminiscences......Page 5966
Shoolery, James N.:High-Resolution NMR: A Dream Come True......Page 5970
Shulman, Robert G.: My Years in NMR......Page 5978
Slichter, Charles P.: Early Days of Magnetic Resonance Studies of Solids......Page 5986
Smith, Ian C. P.: Deuterium NMR: Reflections on its Evolution......Page 5993
Spiess, Hans Wolfgang:Multidimensional Solid State NMR of Polymers......Page 5995
Stejskal, Edward O.:Reminiscences about the Development of Pulsed Field Gradient, Spin-Echo NMR (PFGSE NMR)......Page 6001
Sternhell, S.: Development of NMR Spectroscopy as a Structural Tool......Page 6003
Strange, John H.: Echoes of the Past......Page 6005
Sutcliffe, Leslie H.: A Career in Magnetic Resonance Spectroscopy......Page 6007
Sykes, Brian D.: When Biochemistry became Chemistry......Page 6009
Temussi, Piero Andrea: NMR Studies of Flexible Bioactive Molecules......Page 6010
The Development of NMR......Page 6012
Torchia Dennis A.: A Fortuitous Transformation......Page 6166
Torrey, Henry C.:Precursive and Early Work on NMR......Page 6168
Veeman, Wiebren S.:Personal Reflections on Solid State NMR in the Early Days......Page 6172
Vega, Alexander J.: Beginnings, Vaughan, and Solid State NMR......Page 6173
Vega, Shimon: From Zero Field via Double Quantum to Dressed States......Page 6175
Vold, Robert L.: Reflections......Page 6177
Vold, Regitze R.: Bits and Pieces from My NMR Memoirs......Page 6179
van der Waals, J. H.:Gorter’s Footprints on the Trail That Led to MagneticResonance......Page 6181
Wagner, Gerhard: NMR of Proteins......Page 6185
Warren, Warren S.: The NMR–Optics Connection......Page 6187
Waugh, John S.: Alchemy of Nuclear Spins......Page 6189
Weaver, Harry E.:Historical Comments on the Early Years of Superconducting NMR......Page 6195
Webb, Graham A.: My Developing Interest in NMR Spectroscopy......Page 6197
Wehrli, Felix W.: From Carbon-13 to Quadrupolar Nuclei NMR and Medical Imaging—Reflections......Page 6199
Weitekamp, Daniel P.: Sensitivity Enhancement Through Spin Statistics......Page 6203
Whiffen, David H.:Forty-Nine Years Watching NMR......Page 6204
Williams, R. J. P.: The Use of NMR in Biology:Personal Reflections......Page 6206
Witanowski, Michal: A Short Story about Nitrogen NMR......Page 6208
Woessner, Donald E.: In a Maze in NMR......Page 6210
Wrackmeyer, Bernd: A Personal Retrospect of Multinuclear Ma
