Development of an Effusive Molecular Beam Apparatus

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Daniel Halwidl presents the development of an effusive molecular beam apparatus, which allows the dosing of gases, liquids, and solids in ultra-high vacuum. The apparatus is designed to adsorb precise and reproducible doses to a defined area on metal oxide samples, which is required in Temperature Programmed Desorption and other surface chemistry experiments. The design and the construction of the apparatus is described. The properties of the molecular beam are experimentally confirmed. The beam profile has a core diameter of 3.5 mm and a standard core pressure of 4 x 10-8 mbar, while the background pressure is 4 orders of magnitude lower.

Author(s): Daniel Halwidl (auth.)
Series: BestMasters
Edition: 1
Publisher: Springer Spektrum
Year: 2016

Language: English
Pages: XVIII, 105
Tags: Physical Chemistry; Catalysis

Front Matter....Pages I-XVIII
Introduction....Pages 1-4
Flow of gases....Pages 5-18
Effusive molecular beam sources....Pages 19-23
Molecular Beam....Pages 25-74
Results....Pages 75-88
Summary and outlook....Pages 89-90
Back Matter....Pages 91-105